Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al<sub>2</sub>O<sub>3</sub> Supported Catalyst

Mohammed Sulieman Ali Eltoum; Rufaa Mohamed Osman Nasr; Hager Mohamed Ahmed Omer

doi:doi:10.11648/j.nano.20200802.11

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Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al₂O₃ Supported Catalyst

Mohammed Sulieman Ali Eltoum, Rufaa Mohamed Osman Nasr, Hager Mohamed Ahmed Omer

Published in American Journal of Nano Research and Applications (Volume 8, Issue 2)

Received: 23 March 2020 Accepted: 6 May 2020 Published: 14 May 2020

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Abstract

In this research copper oxide (CuO) nanoparticles were prepared by sol gel method. In this method CuCl₂.2H₂O was used as precursor, the obtained CuO nanoparticles were further supported by alumina to produce copper oxide support on alumina catalyst, the copper oxide nanoparticle and the catalyst were characterized using different analytical techniques such as titrimetric method, x-ray diffraction (XRD), Scanning Electron Microscope (SEM) and the catalyst was applied in the synthesis of tetraethyl orthosilicate (TEOS). The obtained results indicated the formation of copper oxide nanoparticles and copper oxide supported in alumina catalyst in high quality, also the catalyst increased the rate of formation of tetraethyl orthosilicate (TEOS).

Published in	American Journal of Nano Research and Applications (Volume 8, Issue 2)
DOI	10.11648/j.nano.20200802.11
Page(s)	16-21
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2020. Published by Science Publishing Group

Keywords

Copper Oxide, Nano Particles, Sol-Gel, Orthosilicate, Catalyst

References

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[2]	M. Shahmiri, N. A. Zowa Ibrahim, N. Zainuddin, Nilofarasim, B. Bakhtyar, A Zaharim, K Sopian (2013), Preparation and characterization of copper oxide nanoparticles. International Journal of ChemTech Research 9 (3): 2224-3496.
[3]	M. I. El-Nahhal. M. Shehata. Zourab, S. Fawzi, Kodeh, M. Semane, I. G. Florence.(2012), Int. Nano Lett., 2: 62-67.
[4]	Chang. Ya-Nan, Mingyi Zhang, Lin Xia, Jun Zhang, (2012), Materials, 5: 2850-2871.
[5]	H. Wyne Richardson (1997), handbook of copper compounds and applications, USA South Carolina, NY. BASEL. Hong Kong, ISBN 0-8247-8998-9.
[6]	A. H. E. Yousif, O. Yousif, Alhusseinb, A. M. Elgorashi., M. S. Ali and W. I. Eldogdugd. (2016). Synthesis and Characterization of Organic Silicates Using Appropriate Catalysts. International Journal of Innovative Science, Engineering & Technology, 3 (1): 2348-7968.
[7]	D. R. Andersonin, (1974). Analysis of silicones. A. Lee Smith, editor, Wiley-Interscience, New York, Chapter 10.

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APA Style

Mohammed Sulieman Ali Eltoum, Rufaa Mohamed Osman Nasr, Hager Mohamed Ahmed Omer. (2020). Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al2O3 Supported Catalyst. American Journal of Nano Research and Applications, 8(2), 16-21. https://doi.org/10.11648/j.nano.20200802.11

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ACS Style

Mohammed Sulieman Ali Eltoum; Rufaa Mohamed Osman Nasr; Hager Mohamed Ahmed Omer. Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al2O3 Supported Catalyst. Am. J. Nano Res. Appl. 2020, 8(2), 16-21. doi: 10.11648/j.nano.20200802.11

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AMA Style

Mohammed Sulieman Ali Eltoum, Rufaa Mohamed Osman Nasr, Hager Mohamed Ahmed Omer. Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al2O3 Supported Catalyst. Am J Nano Res Appl. 2020;8(2):16-21. doi: 10.11648/j.nano.20200802.11

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@article{10.11648/j.nano.20200802.11,
  author = {Mohammed Sulieman Ali Eltoum and Rufaa Mohamed Osman Nasr and Hager Mohamed Ahmed Omer},
  title = {Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al2O3 Supported Catalyst},
  journal = {American Journal of Nano Research and Applications},
  volume = {8},
  number = {2},
  pages = {16-21},
  doi = {10.11648/j.nano.20200802.11},
  url = {https://doi.org/10.11648/j.nano.20200802.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.nano.20200802.11},
  abstract = {In this research copper oxide (CuO) nanoparticles were prepared by sol gel method. In this method CuCl2.2H2O was used as precursor, the obtained CuO nanoparticles were further supported by alumina to produce copper oxide support on alumina catalyst, the copper oxide nanoparticle and the catalyst were characterized using different analytical techniques such as titrimetric method, x-ray diffraction (XRD), Scanning Electron Microscope (SEM) and the catalyst was applied in the synthesis of tetraethyl orthosilicate (TEOS). The obtained results indicated the formation of copper oxide nanoparticles and copper oxide supported in alumina catalyst in high quality, also the catalyst increased the rate of formation of tetraethyl orthosilicate (TEOS).},
 year = {2020}
}

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TY  - JOUR
T1  - Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al2O3 Supported Catalyst
AU  - Mohammed Sulieman Ali Eltoum
AU  - Rufaa Mohamed Osman Nasr
AU  - Hager Mohamed Ahmed Omer
Y1  - 2020/05/14
PY  - 2020
N1  - https://doi.org/10.11648/j.nano.20200802.11
DO  - 10.11648/j.nano.20200802.11
T2  - American Journal of Nano Research and Applications
JF  - American Journal of Nano Research and Applications
JO  - American Journal of Nano Research and Applications
SP  - 16
EP  - 21
PB  - Science Publishing Group
SN  - 2575-3738
UR  - https://doi.org/10.11648/j.nano.20200802.11
AB  - In this research copper oxide (CuO) nanoparticles were prepared by sol gel method. In this method CuCl2.2H2O was used as precursor, the obtained CuO nanoparticles were further supported by alumina to produce copper oxide support on alumina catalyst, the copper oxide nanoparticle and the catalyst were characterized using different analytical techniques such as titrimetric method, x-ray diffraction (XRD), Scanning Electron Microscope (SEM) and the catalyst was applied in the synthesis of tetraethyl orthosilicate (TEOS). The obtained results indicated the formation of copper oxide nanoparticles and copper oxide supported in alumina catalyst in high quality, also the catalyst increased the rate of formation of tetraethyl orthosilicate (TEOS).
VL  - 8
IS  - 2
ER  -

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Author Information

Mohammed Sulieman Ali Eltoum

Department of Chemistry, Sudan University of Science and Technology, Khartoum, Sudan
Rufaa Mohamed Osman Nasr

Department of Chemistry, Sudan University of Science and Technology, Khartoum, Sudan
Hager Mohamed Ahmed Omer

Chemistry Department, College of Science, Jazan University, KSA

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Plain Text BibTeX RIS

APA Style

Mohammed Sulieman Ali Eltoum, Rufaa Mohamed Osman Nasr, Hager Mohamed Ahmed Omer. (2020). Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al2O3 Supported Catalyst. American Journal of Nano Research and Applications, 8(2), 16-21. https://doi.org/10.11648/j.nano.20200802.11

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ACS Style

Mohammed Sulieman Ali Eltoum; Rufaa Mohamed Osman Nasr; Hager Mohamed Ahmed Omer. Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al2O3 Supported Catalyst. Am. J. Nano Res. Appl. 2020, 8(2), 16-21. doi: 10.11648/j.nano.20200802.11

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AMA Style

Mohammed Sulieman Ali Eltoum, Rufaa Mohamed Osman Nasr, Hager Mohamed Ahmed Omer. Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al2O3 Supported Catalyst. Am J Nano Res Appl. 2020;8(2):16-21. doi: 10.11648/j.nano.20200802.11

Copy | Download

@article{10.11648/j.nano.20200802.11,
  author = {Mohammed Sulieman Ali Eltoum and Rufaa Mohamed Osman Nasr and Hager Mohamed Ahmed Omer},
  title = {Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al2O3 Supported Catalyst},
  journal = {American Journal of Nano Research and Applications},
  volume = {8},
  number = {2},
  pages = {16-21},
  doi = {10.11648/j.nano.20200802.11},
  url = {https://doi.org/10.11648/j.nano.20200802.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.nano.20200802.11},
  abstract = {In this research copper oxide (CuO) nanoparticles were prepared by sol gel method. In this method CuCl2.2H2O was used as precursor, the obtained CuO nanoparticles were further supported by alumina to produce copper oxide support on alumina catalyst, the copper oxide nanoparticle and the catalyst were characterized using different analytical techniques such as titrimetric method, x-ray diffraction (XRD), Scanning Electron Microscope (SEM) and the catalyst was applied in the synthesis of tetraethyl orthosilicate (TEOS). The obtained results indicated the formation of copper oxide nanoparticles and copper oxide supported in alumina catalyst in high quality, also the catalyst increased the rate of formation of tetraethyl orthosilicate (TEOS).},
 year = {2020}
}

Copy | Download

TY  - JOUR
T1  - Preparation and Characterization of CuO Nano Particles Using Sol-Gel Method and Its Application as CuO/ Al2O3 Supported Catalyst
AU  - Mohammed Sulieman Ali Eltoum
AU  - Rufaa Mohamed Osman Nasr
AU  - Hager Mohamed Ahmed Omer
Y1  - 2020/05/14
PY  - 2020
N1  - https://doi.org/10.11648/j.nano.20200802.11
DO  - 10.11648/j.nano.20200802.11
T2  - American Journal of Nano Research and Applications
JF  - American Journal of Nano Research and Applications
JO  - American Journal of Nano Research and Applications
SP  - 16
EP  - 21
PB  - Science Publishing Group
SN  - 2575-3738
UR  - https://doi.org/10.11648/j.nano.20200802.11
AB  - In this research copper oxide (CuO) nanoparticles were prepared by sol gel method. In this method CuCl2.2H2O was used as precursor, the obtained CuO nanoparticles were further supported by alumina to produce copper oxide support on alumina catalyst, the copper oxide nanoparticle and the catalyst were characterized using different analytical techniques such as titrimetric method, x-ray diffraction (XRD), Scanning Electron Microscope (SEM) and the catalyst was applied in the synthesis of tetraethyl orthosilicate (TEOS). The obtained results indicated the formation of copper oxide nanoparticles and copper oxide supported in alumina catalyst in high quality, also the catalyst increased the rate of formation of tetraethyl orthosilicate (TEOS).
VL  - 8
IS  - 2
ER  -

Copy | Download